American Association for Aerosol Research - Abstract Submission

AAAR 34th Annual Conference
October 12 - October 16, 2015
Hyatt Regency
Minneapolis, Minnesota, USA

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Traceable Calibration of Detection Efficiencies of Optical Particle Counters using Inkjet Aerosol Generator

KENJIRO IIDA, Kensei Ehara, Hiromu Sakurai, AIST

     Abstract Number: 377
     Working Group: Instrumentation and Methods

Abstract
National institute of advanced industrial science and technology (AIST), Japan, launched a calibration service for evaluating the counting efficiencies of optical particles counters (OPCs). The values are evaluated using a monodisperse aerosol generator which can precisely control the particle generation rates. The device is called AIST-inkjet aerosol generator (AIST-IAG) which is the primary standard for particle count rates of OPCs at AIST. In the menu for the calibration serve, particle count rates range from 10 /s to 100 /s, particle diameter ranges from 0.5 um to 10 um, sampling flowrates of OPC, Q, range from 0.3 L/min to 30 L/min, and particle materials are sodium chloride, ammonium sulfate, and water soluble ionic liquid. Aerosol flowrate of AIST-IAG cannot exceed 1 L/min; therefore, when the value of Q is greater than 1 L/min, clean sheath-air is added at a sampling inlet to complement the value of Q. The value of Q can be measured traceably upon request to express the values of E in terms of particle number concentration. For example, the ranges of concentrations are 0.02-0.2 /cm3 and 2-20 /cm3 when the value of Q are 30 L/min and 0.3 L/min, respectively. In this presentation calibration results for four OPCs whose sampling flowrates are 0.3, 0.5, 2.83, and 28.3 L/min. The expanded uncertainties of the counting efficiencies, U(k=2), were evaluated in the plateau region of the size-dependent counting efficiency curve when the particle generation rate of the AIST-IAG was fixed at 100 /s. The values of U(k=2) based on particle count rates ranged from 0.0025 to 0.0027. In terms of the particle number concentration the values ranged from 0.0044 to 0.0046. The results demonstrates that the AIST-IAG can calibrate OPCs accurately. This calibration method can potentially become an alternative to the calibration methods documented in ISO 21501-4 or JIS B 9921.